Contact Manager: Emma Song Email Address: emma@coreychem.com
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Items |
Specifications |
Test Result |
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Appearance |
Colorless or light yellow oily liquid |
Colorless oily liquid |
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Identification |
IR: chromatograph conforms to the characteristic peak of R.S. |
Conforms |
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HPLC: retention time of sample should be concordant with that of reference standard. |
Conforms |
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Water |
≤0.5% |
0.10% |
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Ignition residue |
≤0.2% |
0.03% |
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Related substances (HPLC) |
3-AMINOSTYRENE |
≤0.01% |
N.D. |
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4-(3-AMINOPHENYL)-2-METHYL-3-BUTYN-2-OL |
≤0.15% |
0.03% |
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3-Bromoaniline |
≤0.05% |
0.01% |
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Max. individual impurity |
≤0.15% |
0.01% |
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Total impurities |
≤1.0% |
0.06% |
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Purity |
≥99.0% |
99.94% |
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Assay |
98.0%-102.0% |
100.3% |
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Residual solvent |
Methanol |
≤3000ppm |
20.8ppm |
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Ethanol |
≤5000ppm |
N.D. |
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Methylene chloride |
≤600ppm |
N.D. |
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Toluene |
≤890ppm |
463.4ppm |
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Acetone |
≤5000ppm |
1304.2ppm |
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| Product Name: | 3-Ethynylaniline |
| Synonyms: | M-ETHYNYLANILINE;M-AMINOPHENYL ACETYLENE;3-AMINOPHENYLACETYLENE;3-ETHYNYLBENZENEAMINE;3-ETHYNYL-PHENYLAMINE;3-ETHYNYLANILINE;Benzenamine, 3-ethynyl-;3-ethynyl-benzenamin |
| CAS: | 54060-30-9 |
| MF: | C8H7N |
| MW: | 117.15 |
| EINECS: | 258-944-6 |
| Melting point | 27°C |
| Boiling point | 92-93 °C (2 mmHg) |
| density | 1.04 |
| refractive index | 1.614-1.616 |
| Fp | 138 °F |
| storage temp. | 2-8°C |
| solubility | Acetonitrile (Slightly), Chloroform (Slightly), DMSO (Slightly) |
| form | Liquid |
| pka | 3.67±0.10(Predicted) |
| color | Clear yellow to brown |
| Specific Gravity | 1.12 |
| Water Solubility | Insoluble in water. |
| BRN | 2935417 |
| Stability: | Light Sensitive |
| Uses | Reagent in the preparation of a labelled metabolite of Erlotinib (E625000). |
| Uses | 3-Aminophenylacetylene is used as a pharmaceutical intermediate. |
